Chromoly Steel Factory – Certified Reference Material – Shandong Institute of Metallurgical Science
Chromoly Steel Factory – Certified Reference Material – Shandong Institute of Metallurgical Science Detail:
Table 1. Certified Values for ZBK 306 (Mass Fraction %)
Number |
Elements |
TFe |
FeO |
SiO2 |
Al2O3 |
CaO |
MgO |
ZBK 306 |
Certified Values |
65.66 |
0.54 |
1.92 |
1.64 |
0.056 |
0.102 |
Uncertainty |
0.17 |
0.06 |
0.04 |
0.04 |
0.006 |
0.008 |
|
Number |
Elements |
S |
P |
Mn |
Ti |
K2O |
Na2O |
ZBK 306 |
Certified Values |
0.022 |
0.060 |
0.135 |
0.048 |
0.018 |
0.007 |
Uncertainty |
0.001 |
0.002 |
0.003 |
0.002 |
0.002 |
0.002 |
Table 2. Analysis methods
Composition |
Method |
TFe |
Titanium(III) chloride reduction potassium dichromate titration method |
FeO |
Potassium dichromate titration methodThe potentiometric titrimetric method |
SiO2 |
Perchloric acid dehydration gravimetric methodThe silicomolybdic blue spectrophotometric methodICP-AES |
Al2O3 |
Complexometric titration methodThe chrome azurol S photometric methodICP-AES |
CaO |
ICP-AESAAS |
MgO |
ICP-AESAAS |
S |
Barium sulfate gravimetric methodThe eombustion iodometric method for the determination of sulfur content |
P |
Bismuth phosphomolybdate blue spectrophotometric methodICP-AES |
Mn |
Potassium periodate spectrophotometric methodICP-AESAAS |
Ti |
Diantipyryl methane photometric methodICP-AES |
K2O |
ICP-AES AAS |
Na2O |
ICP-AES AAS |
Expiration of certification: The certification of this CRM is valid until December 1, 2028.
Table 3. Methods for homogeneity testing
Composition |
Analysis methods |
Minimum sample (g) |
TFe |
Titanium(III) chloride reduction potassium dichromate titration method |
0.2 |
FeO |
Potassium dichromate titration method |
0.2 |
SiO2, Al2O3, CaO, MgO |
ICP-AES |
0.1 |
Mn, Ti |
ICP-AES |
0.2 |
P, K2O, Na2O |
ICP-AES |
0.5 |
S |
The eombustion iodometric method for the determination of sulfur content |
0.5 |
The certified reference material is packed in glass bottles with plastic covers. The net weight is 70 g each. It is suggested to keep dryness when stored. The certified reference material should be dried at 105℃ for 1 hour before use, then it should be taken out and cooled to room temperature.
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By Dorothy from France - 2017.07.28 15:46
The company keeps to the operation concept "scientific management, high quality and efficiency primacy, customer supreme", we have always maintained business cooperation. Work with you,we feel easy!
By Ivy from Holland - 2018.12.30 10:21